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  Silica
 
Method

References: APHA Standard Methods, 20th ed., pp. 4-158, Method 4500-SiO2 D (1998). ASTM D 859-00, Silica in Water. USEPA Methods for Chemical Analysis of Water and Wastes, Method 370.1 (1983).

Silica (SiO2) is the oxide of silicon, the second most abundant element in the earth’s crust. Silica is present as silicates in most natural waters. Typical concentrations lie between 1 and 30 mg/L. Higher concentrations may exist in brackish waters and brines. The silica content of water should be determined prior to its use in a variety of industrial applications. Silica can form a harmful scale on equipment and heat transfer surfaces, particularly steam turbine blades.

CHEMetrics’ test method determines molybdate reactive silica. The heteropoly blue chemistry is employed. Silica reacts with ammonium molybdate under acidic conditions to produce heteropoly acids, which are then reduced to form a blue color. Phosphate interferences are masked with the addition of citric acid. Results are expressed as ppm (mg/L) SiO2.
 
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  Visual Kits
0-0.20 ppm
0.02 ppm / Method: Heteropoly Blue
  Cat#
ULR CHEMets Kit K-9011

ULR CHEMets Refill, 30 ampoules, Shelf-life 2 monthsR-9011

Neutralizer Solution Pack, six 10 mL bottles, Shelf-life 2 yearsA-9000

Activator Solution Pack, six 20 mL bottles, Shelf-life 2 yearsA-9001

Comparator, Shelf-life 2 years: 0, 0.02, 0.04, 0.06, 0.08, 0.12, 0.16, 0.20 ppmC-9011

Kit comes in a plastic case and contains everything needed to perform 30 tests: Refill, Comparator, Neutralizer Solution, Activator Solution, 25 mL sample cup, sample cup top, instructions, and MSDS.
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0-1 & 1-10 ppm
0.05 ppm / Method: Heteropoly Blue
  Cat#
CHEMets Kit K-9010

CHEMets Refill, 30 ampoules, Shelf-life 11 monthsR-9010

Neutralizer Solution Pack, six 10 mL bottles, Shelf-life 2 yearsA-9000

Activator Solution Pack, six 20 mL bottles, Shelf-life 2 yearsA-9001

Low Range Comparator, Shelf-life 2 years: 0, 0.1, 0.2, 0.3, 0.4, 0.6, 0.8, 1.0 ppmC-9001

High Range Comparator, Shelf-life 2 years: 1, 2, 3, 4, 5, 6, 7, 8, 10 ppmC-9010

Kit comes in a plastic case and contains everything needed to perform 30 tests: Refill, Low and High Range Comparators, Neutralizer Solution, Activator Solution, 25 mL sample cup, sample cup top, instructions, and MSDS.
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  Instrumental Kits
V-2000: 0.50-10.00 ppm / Spec: 0.25-4.00 ppm
Heteropoly Blue
  Cat#
Vacu-vials Kit K-9003

Kit comes in a cardboard box and contains everything needed to perform 30 tests: thirty ampoules, Neutralizer Solution, Activator Solution, 25 mL sample cup, sample cup top, ampoule blank, instructions, calibration table, and MSDS.
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Kit Components common to Silica
Description Cat#

Sample Cup Pack, 25 mL (6 ea)A-0013

Sample Cup Top Pack for 25 mL Cup (6 ea)A-0014

Ampoule Blank Pack (5 ea)A-0023
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