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  Glycol
 
Method

References: Purpald® developed by Aldrich Chemical Company.

Ethylene glycol and propylene glycol are the primary ingredients in commercially-available antifreezes. They are used with various corrosion inhibitors to protect metal surfaces in cooling water systems.

CHEMetrics’ glycol test kits, which employ a chemistry perfected by CHEMetrics, are used to monitor potable waters for contamination from glycol originating in cooling systems.

Stricter limits for stormwater effluent glycol discharges are expected from the USEPA. In addition to the glycol recycling operations, monitoring the efficiency of recovery and collection systems is crucial.

In the colorimetric chemistry, periodic acid oxidizes ethylene glycol and/or propylene glycol to formaldehyde, which reacts with Purpald in alkaline solution. Visual and instrumental test kits are available that report test results in either ppm (mg/L) ethylene or propylene glycol. Correction factors are supplied with all kits to convert test results to the alternate glycol form.

This test requires much less time to perform and involves fewer manipulations than the standard chromotropic acid procedure.

Shelf-life: six months. We recommend stocking quantities that will be used within five months. Refrigeration will dramatically increase the shelf-life of these products.
 
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  Visual Kits
1-15 ppm as ethylene glycol
1 ppm / Method: Purpald-Periodate
  Cat#
CHEMets Kit K-4815

CHEMets Refill, 30 ampoules, Shelf-life 5 monthsR-4815

Activator Solution Pack, six 10 mL bottles, Shelf-life 2 yearsA-4400

Activator Solution Pack, six 20 mL bottlesA-4401

Activator Solution Pack, six 10 mL bottles, Shelf-life 2 yearsA-4402

Comparator, Shelf-life 2 years: 1, 2, 3, 4, 5, 6, 8, 10, 15 ppmC-4815

Kit comes in a plastic case and contains everything needed to perform 30 tests (except distilled water): Refill, Comparator, Activator Solutions, 25 mL sample cup, sample cup top, instructions, and MSDS.
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1000-15,000 ppm as ethylene glycol
1000 ppm / Method: Purpald-Periodate
  Cat#
VACUettes Kit K-4815C

VACUettes Refill, 30 ampoules, Shelf-life 5 monthsR-4815C

Activator Solution Pack, six 10 mL bottles, Shelf-life 2 yearsA-4404

Activator Solution Pack, six 20 mL bottlesA-4401

Activator Solution Pack, six 10 mL bottles, Shelf-life 2 yearsA-4402

Comparator, Shelf-life 2 years: 1000, 2000, 3000, 4000, 5000, 6000, 8000, 10,000, 15,000 ppmC-4815C

Kit comes in a plastic case and contains everything needed to perform 30 tests (except distilled water): Refill, Comparator, Activator Solutions, dilutor snapper cup, micro test tube, instructions, and MSDS.
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  Instrumental Kits
0.60-10.00 ppm as ethylene glycol
Purpald-Periodate
  Cat#
Vacu-vials Kit, Shelf-life 5 months K-4403

Kit comes in a cardboard box and contains everything needed to perform 30 tests (except distilled water): thirty ampoules, Activator Solutions, 25 mL sample cup, sample cup top, ampoule blank, instructions, calibration table, and MSDS.
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5-65 ppm as propylene glycol
Purpald-Periodate
  Cat#
Vacu-vials Kit, Shelf-life 5 months K-4423

Kit comes in a cardboard box and contains everything needed to perform 30 tests (except distilled water): thirty ampoules, Activator Solutions, Stabilizer Solution, 25 mL sample cup, sample cup top, ampoule blank, instructions, calibration table and MSDS.
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Kit Components common to Glycol
Description Cat#

Sample Cup Pack, 25 mL (6 ea)A-0013

Sample Cup Top Pack for 25 mL Cup (6 ea)A-0014

Micro Test Tube Pack (10 ea)A-0015

Dilutor Snapper Cup Pack (6 ea)A-0018

Ampoule Blank Pack (5 ea)A-0023

Sample Cup & Cap Pack, 50 mL (6 ea)A-0058

Syringe Pack, 10 mL (6 ea)A-0104
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Email: sales@watertestsystems.com.au
Watertest Systems Pty Ltd 2006
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